Example 1. MEKO-end-capped PU Coating

1) Preparation of MEKO-end-capped PU prepolymer solution

Formulation:

		Parts(w/w)
a.	α,α,α',α'-Tetramethyl Xylylene Diisocyanate	259
b.	Carbitol Acetate	400
c.	Trimethylolpropane	28
d.	Polybutanol	212
e.	Dibutyltin Dilaurate	0.1
f.	MEKO	101

Add ingredients a,b, c,d and e into a reactor fitted with a stirrer, heater, thermometer and gas inlet. Heat to 80~100 while stirring under nitrogen and keep for 3hr to allow max. PU prepolymer yield, that is NCO% reaches 8.9%. Add MEKO (ingredient f) into the solution and react at 60~80 for 3hr until NCO peaks disappear by IR detection. Thus MEKO end-capped PU prepolymer solution, with 60% of solid content, is obtained.

2) Preparation of the coating

Formulation:

g.	MEKO end-capped PU prepolymer solution	100
h.	Carbon Black	1
i.	Titanium Dioxide	5
j.	Calcium Carbonate	80
k.	Aromatic Naphtha (bp. 100~200)	30

Place the above ingredients in a mixer, and mix thoroughly to achieve a uniform suspension.

Characteristics and Use:

1. High adhesion, impact resistance and storage stability.
2. Suitable for galvanized steel surface, automotive, etc.
3. Recommended to apply by air spray; bake at 120 for 15min; film thickness 20μm. It can also be applied by brush, roller, blade and E-coating. ple 2. Waterborne Exterior Coating

Formulation:

Water	8.33
Soy Lecithin Emulsion (Centromix LP-1421)	9.0
Linaqua	8.10
Titanium Dioxide	34.99
Al powder or Zinc Oxide 427W	46.7
Linseed Oil	22.46
Talc	23.75
Phenyl Alkylsulfonate	21.65
Water	8.33
Linaqua	8.10
SynvarexlA-5-97	7.7
6% Cobalt Caprylate	7.4
6% Magnesium Naphthenate	7.97
24% Cobalt Naphthenate	9.7
8% Zinc Naphthenate	8.00
MEKO	7.65
Water	8.33

Disperse Centromix LP-1421 in water. Add Linaqua slowly while stirring. Then add the next 5 ingredients in sequence as listed above. Mill the resulting solution to 4 Hegman (50.00 um). Add the remaining ingredients in sequence and stir thoroughly.

Characteristics and Use:

1. Exterior masonry coating with glaze finish.
2. Excellent weather resistance.

Example 3. Solventborne Interior Coatng

Formulation 1: Low-gloss white alkyd coating

Titanium Dioxide OR-540	34.15
Calcium Carbonate	22.57
Zinc Oxide (Kaclox 515)	46.70
5% Calcium Naphthenate	7.90
Beckosol P-470-60 Alkyd Resin	7.73
Solvent Oil (bp. 150~200)	6.53
Levelling Agent	7.15
Solvent Oil (bp. 150~200)	6.52
6% Colbalt Naphthenate	8.16
MEKO	7.65

Place the first 6 ingredients in a colloid mill and reduce the particle size to 6 Hegman (25.00um). Add the remaining ingredients in sequence while stirring and mix thoroughly.

Characteristics and Use:

1. Interior wood and concrete coating.
2. High wear resistance.

Formulation 2: White glossy lacquer

Titanium Dioxide R-750	34.15
Zinc Oxide Kadox515	46.70
4% Calcium Naphthenate	7.85
Thixcin	8.51
Backosol P-470-70 Alkyd Resin	7.86
Solvent Oil (bp. 150~200)	6.52
Backosol P-470-70 Alkyd Resin	7.86
Solvent Oil	6.52
6% Colbalt Naphthenate	7.95
Violet Dispersing Agent	8.50
MEKO	7.65

Place the first 6 ingredients in a colloid mill and reduce the particle size to 6 Hegman (25.00um). Add the remaining ingredients in sequence while stirring and mix thoroughly.

Characteristics and Use:

1. Hard surface coating.
2. High wear and aging resistance.

Example 4. White Chlorinated Rubber/Alkyd Lacquer

Formulation:

	I Parts (w/w)	II Parts (w/w)
5~20mpa.S Chlorinated Rubber	-	-
Medium-oil Soy Alkyd (70%)	8.5	8.9
Long-oil Linseed Alkyd (70%)	30.4	27.0
Titanium Dioxide (Rutile)	18.4	19.40
Cobalt Naphthenate	0.2	0.2
Lead Naphthenate	0.4	0.4
MEKO	0.1	0.1
Petroleum Solvent	8.0	11.0
Aromatic Solvent	34.0	33.0
Total	100	100

Example 5. Chlorinated Rubber Road Paint

Formulation:

	I Parts (w/w)	II Parts (w/w)	III Parts (w/w)
20mpa.s Chlorinated Rubber	8.6	6.1	6.5
Long-oil Alkyd (60%)	6.6	16.5	14.0
Chlorinated Paraffin (70%)	-	-	-
Chlorinated Paraffin (42%)	6.4	-	-
Titanium Dioxide (Rutile)	17.1	17.6	9.6
Zinc Oxide	4.3	-	-
Blanc Fix	-	14.0	19.2
Talc	12.0	14.1	9.6
Calcium Carbonate Heavy	10.8	-	9.6
Modified Bentonite	0. 5	0.5	0.5
Epichlorohydrin	0. 3	0.2	0.5
Cobalt Naphthenate	0.1	0.2	0.1
Lead Naphthenate	0.2	0.4	0.2
Butanone	29.8	-	-
Toluene	-	30.1	20.7
Ethyl Acetate	3.0	-	-
MEKO	0.3	0.3	0.3
Total	100	100	100

Example 6. Alkyd Lacquer

Formulation (parts w/w):

	Black	Red	Green	Light Grey	Sky Blue	White
Alkyd (50%)	88.3	79.8	72.3	70.00	70.25	66.40
Carbon Black (Hard)	2.00	-	-	-	-	-
Titanium Dioxide (Rutile)	-	-	-	19.20	18.80	25.40
Lemon Yellow	-	-	11.40	0.39	-	-
Iron Blue	-	-	2.40	0.20	1.20	-
Carbon Black (Soft)	-	-	-	0.25	-	-
Toluidine Red	-	8.00	-	-	-	-
French Blue	-	-	-	-	-	0.18
Medium Chrome Yellow	-	-	1.9	-	-	-
Lead Oxide	0.08	0.1	0.07	0.07	0.06	0.07
Lead Naphthenate (12%)	1.20	1.5	1.40	2.00	2.00	2.00
Cobalt Naphthenate (3%)	1.2	0.30	0.40	0.20	0.60	0.80
Manganese Naphthenate (3%)	0.60	0.60	0.40	0.80	0.60	0.20
Zinc Naphthenate (3%)	0.78	0.80	1.10	0.94	0.80	0.80
Calcium Naphthenate (2%)	0.85	0.90	0.82	1.24	1.20	1.20
Silicone Oil (1%)	-	-	0.40	0.40	0.40	-
MEKO(50%)	0.41	0.41	0.41	0.41	0.41	0.41
Xylene
PVC, %	2.69	12.4	9.2	15.9	14.4	16.4